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ISO 23631:2006Published

Water quality — Determination of dalapon, trichloroacetic acid and selected haloacetic acids — Method using gas chromatography (GC-ECD and/or GC-MS detection) after liquid-liquid extraction and derivatization

Qualité de l'eau — Dosage du dalapon, de l'acide trichloroacétique et d'acides haloacétiques selectionnés — Méthode par chromatographie en phase gazeuse (détection CG-DCE et/ou CG-SM) après extraction liquide-liquide et dérivatisation

Abstract / scope

ISO 23631:2006 specifies a method for the determination of dalapon, trichloroacetic acid (TCA) and selected haloacetic acids in ground water and drinking water by gas chromatography (GC-ECD and/or GC-MS detection) after liquid-liquid-extraction and derivatization using diazomethane. Depending on the matrix, the method is applicable to a concentration range from 0,5 to 10 micrograms per litre. The validated reporting limit of TCA and dalapon is about 0,05 micrograms per litre. Detection by electron-capture detector (ECD) in general leads to lower detection limits. Detection by mass spectrometry (MS) allows analyte identification.