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ISO 17052:2007Published

Rubber, raw — Determination of residual monomers and other volatile low-molecular-mass compounds by capillary gas chromatography — Thermal desorption (dynamic headspace) method

Caoutchouc brut — Détermination des monomères résiduels et autres composés volatils de masse moléculaire faible par chromatographie en phase gazeuse sur colonne capillaire — Méthode par désorption thermique (espace de tête dynamique)

Abstract / scope

ISO 17052:2007 specifies a method for the determination of residual monomers and other volatile low-molecular-mass compounds in raw rubber by capillary column gas chromatography using a thermal desorption (also known as dynamic headspace) method. It includes a generic section that is applicable to all types of raw rubber and two annexes specific to particular rubber types.

This method has the advantages of not requiring a solvent, of concentrating the volatile compounds and of introducing them to the chromatograph in a very precise manner.

The compounds found in the raw rubber which are to be determined are defined as residual monomers, solvents and other low-molecular-mass compounds in the boiling point range of C4 to C12 hydrocarbons.

NOTE The limit of detection is 1 microgram per gram.