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IEC 62321-11:2023Published

Determination of certain substances in electrotechnical products — Part 11: Tris (2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS)

Détermination de certaines substances dans les produits électrotechniques — Partie 11: Phosphate de tris (2-chloroéthyle) (TCEP) dans les plastiques par chromatographie en phase gazeuse-spectrométrie de masse (GC-MS) et chromatographie liquide-spectrométrie de masse (LC-MS)

Abstract / scope

This part of IEC 62321 specifies two different techniques for the determination of tris(2‑chloroethyl) phosphate (TCEP) in plastics, the GC-MS or LC-MS method, both of which are applicable to quantitative analysis.

These two techniques are applicable to use with polyurethane, polyvinylchloride, and polyethylene materials containing TCEP between 200 mg/kg to 2 000 mg/kg.

These test methods do not apply to plastic materials having a processing temperature higher than 230 °C.

GC-MS using a pyrolyser/thermal desorption accessory (Py/TD-GC-MS) technique is described in Annex A and can be used for the screening of TCEP in plastics.

NOTE TCEP starts thermal decomposition at approximately 230 °C. Polymer types that have a processing temperature into shapes of plastics (e.g. pellets, moulded parts or sheets) not exceeding the decomposition temperature can contain TCEP.